5 Gallon Moonshine Mash Recipe

We’ve always been fascinated by moonshine’s rich history as a homemade American spirit born from ingenuity and rebellion. Our 5 Gallon Moonshine Mash Recipe brings that tradition to your kitchen offering a simple way to craft a smooth batch that’s perfect for gatherings or personal enjoyment.

It’s not just about the thrill of distillation—it’s about connecting with age-old techniques while ensuring safety and quality. We’ll walk you through the essentials so you can create your own flavorful mash with confidence and ease.

Ingredients

In our 5 Gallon Moonshine Mash Recipe, we select high-quality ingredients that form the foundation for a smooth, flavorful mash. These components, sourced for their role in fermentation and flavor development, ensure a traditional yet safe brewing experience.

To prepare your mash, gather the following ingredients in the order they are typically used during the process. We emphasize precise measurements for optimal results, as accuracy directly impacts the mash’s efficiency and taste.

  • Water: 5 gallons of filtered or distilled water – use this as the base to dissolve and hydrate other elements, ensuring it’s at room temperature for even mixing.
  • Cracked Corn: 8.5 pounds of coarsely cracked corn – this primary grain provides the starchy backbone, offering a sweet, earthy flavor that forms the mash’s core during the initial soaking phase.
  • Malted Barley: 1.5 pounds of malted barley – added next for its natural enzymes that convert starches to sugars, contributing a nutty, malty depth that enhances fermentation.
  • Rye Grain: 1 pound of whole rye grain – incorporate this after the base grains to introduce spicy, robust notes that balance the sweetness and aid in texture.
  • Yeast: 2 packets (about 10 grams) of distiller’s yeast – introduce at the fermentation stage for its vigorous activity, producing a clean, aromatic alcohol profile with fruity undertones.
  • White Sugar: 5 pounds of granulated white sugar (optional for a sweeter mash) – dissolve this later if boosting alcohol content, as it ferments quickly to add a clean, neutral sweetness.
  • Yeast Nutrient: 1 tablespoon of yeast nutrient blend – mix in just before pitching the yeast to promote healthy fermentation, preventing off-flavors and ensuring robust activity.

Note: Always prioritize fresh, high-quality ingredients to avoid contaminants, which can affect the mash’s sensory appeal – from the grainy aroma of the corn to the bubbly vigor of active yeast. If scaling for larger batches, adjust measurements proportionally for consistency.

Equipment Needed

To craft our 5 Gallon Moonshine Mash Recipe successfully, we need the right equipment to ensure safe, efficient fermentation and distillation. Building on our ingredient selection, this setup helps us maintain precise control over temperature, sanitation, and the overall process for optimal flavor and quality.

Here’s a detailed list of essential equipment, organized by the order of use in the recipe. We recommend high-quality, food-grade items to prevent contamination and achieve the best results.

  • Fermentation Bucket (5-gallon capacity): A large, plastic or glass bucket with a lid for holding our mash during fermentation. We use this to mix ingredients like cracked corn and water, ensuring it’s airtight to allow gases to escape without letting in contaminants.
  • Airlock and Stopper: This vital component fits into the fermentation bucket’s lid and allows carbon dioxide to vent while keeping oxygen out, preventing off-flavors in our mash.
  • Hydrometer: A tool for measuring the specific gravity of our liquid before and after fermentation, helping us track alcohol potential accurately. We always sanitize it thoroughly for reliable readings.
  • Thermometer (Digital or Floating): Essential for monitoring mash temperature, which should stay between 140-160°F during initial heating to activate enzymes without killing the yeast.
  • Large Stock Pot (At Least 5-Gallons): Used for heating and mashing ingredients, this sturdy pot ensures even cooking and easy stirring of our rye grain and malted barley mixture.
  • Long-Handled Stirring Spoon or Paddle: Made of stainless steel or food-grade plastic, this helps us mix the mash thoroughly, promoting even fermentation and extracting maximum flavors from our grains.
  • Strainer or Mesh Bag: For separating solids from liquids after mashing, allowing us to strain out grains and achieve a clear wort for fermentation.
  • Sanitizer Solution (e.g., Star San or Bleach Mixture): Not equipment per se, but a must-have item for cleaning all tools before use—critical for avoiding bacterial growth that could ruin our batch.

For quick reference, here’s a table comparing key equipment specifications to help us choose based on batch size:

Equipment Item Recommended Size/Capacity Key Function Why It’s Important for Our 5-Gallon Batch
Fermentation Bucket 5-6 gallons Fermentation container Handles full volume without overflow, ensuring stable fermentation.
Hydrometer Standard (0-200 proof) Measures sugar and alcohol Provides precise data to gauge fermentation progress and final ABV.
Thermometer -50°F to 300°F range Temperature monitoring Maintains ideal mash conditions to prevent yeast stress or incomplete conversion.

With this equipment ready, we’re set to move forward confidently and create a smooth, flavorful 5-gallon moonshine mash.

Instructions

Now that we have gathered our high-quality ingredients and essential equipment, we guide you through the precise steps to craft a smooth 5 Gallon Moonshine Mash. Follow these instructions carefully to ensure safety, flavor, and success in your distillation journey.

Prepare the Mash

To start, we combine our grains and water to create a nutrient-rich mash base that sets the foundation for fermentation. Begin by sanitizing all equipment with the sanitizer solution to prevent contamination.

  • Heat the water: In a large stock pot, bring 3 gallons of filtered water to a boil over medium heat. Once boiling, reduce to a simmer and add 2.5 pounds of cracked corn, stirring continuously for 15 minutes until the mixture thickens and releases a hearty, earthy aroma.
  • Add the grains: Gradually incorporate 2 pounds of malted barley and 1 pound of rye grain, stirring vigorously to avoid clumping. Maintain a temperature of 150-160°F (use your thermometer to monitor) for 60 minutes. This step allows the starches to convert to sugars, creating a sweet, malty liquid that we’ll vividly describe as having a warm, grainy scent that fills the kitchen.
  • Cool the mash: Remove the pot from heat and add the remaining 2 gallons of filtered water to cool it down to around 70-80°F. If needed, use an ice bath. Stir in 1 packet of distiller’s yeast, 1 teaspoon of yeast nutrient, and optionally 2 pounds of white sugar for extra fermentable sugars. The mixture should now have a smooth, slightly sweet texture—aim for a consistency like thick porridge.

Ferment the Mash

With the mash prepared, we now focus on fermentation, where yeast transforms sugars into alcohol in a lively, bubbling process that builds the mash’s character.

  • Transfer to fermenter: Pour the cooled mash into the fermentation bucket using a strainer to remove solids, ensuring a clean liquid for optimal results. Seal the bucket with the airlock and stopper, filling the airlock with water to allow CO2 escape while keeping contaminants out.
  • Pitch the yeast: If not already added, sprinkle 1 packet of distiller’s yeast over the mash surface and gently stir. Maintain a stable temperature of 68-72°F in a dark, cool area—use your thermometer to check regularly. Fermentation typically begins within 12-24 hours, marked by vigorous bubbling and a fruity, yeasty aroma that signals active transformation.
  • Monitor progress: Use the hydrometer to track the specific gravity; start at around 1.050 and aim for it to drop to 1.000 or below after 7-14 days. Create a simple table below to log key data points for accuracy:
Day Specific Gravity Temperature (°F) Observations
1 1.050 70 Bubbles starting; yeasty smell
3 1.030 72 Active foaming; sweet-fruity scent
7 1.010 68 Bubbling slows; flavor mellowing
14 1.000 or below 70 Fermentation complete; clear liquid

Once the bubbling stops and the hydrometer reading stabilizes, your mash is ready for the next stage—revel in the satisfying transformation from sweet mash to potent wash.

Distill the Moonshine

Finally, we distill the fermented mash to produce clear, potent moonshine, emphasizing safety and precision to yield a smooth spirit with rich flavors.

  • Set up distillation: Transfer the fermented mash (now called wash) to your still, ensuring all connections are secure. Heat gradually to 173-212°F, the boiling point of alcohol, and collect the distillate in a clean container—watch for the first drops, which carry a sharp, potent aroma indicating pure ethanol.
  • Collect fractions: Divide the run into heads (first 5-10% discarded for safety due to harmful compounds), hearts (the desirable middle run with smooth, flavorful notes), and tails (last portion, which can be saved for future batches). Use your thermometer to maintain 173-185°F for the hearts, capturing 1-2 gallons of high-quality spirit—the liquid should taste clean and fiery with subtle grain undertones.
  • Store and age: Cool the distilled moonshine to room temperature, then dilute with filtered water to reach 80-100 proof if desired. Bottle in airtight containers and age for at least 2 weeks in a cool, dark place to mellow flavors, resulting in a crisp, inviting spirit perfect for sipping or sharing. Always prioritize safety by testing with a hydrometer and never consume without proper verification.

Make-Ahead Instructions

As we guide you through crafting your 5 Gallon Moonshine Mash Recipe, preparing elements in advance ensures a seamless process while maintaining safety and flavor integrity. We focus on steps that allow you to handle time-sensitive tasks ahead of time, building on our previous discussions of fermentation and distillation.

Preparing the Mash Base Ahead

To optimize your brewing schedule, we recommend making the mash base up to 24 hours in advance. This step lets flavors develop without rushing the process. Begin by gathering your ingredients from our earlier list—filtered water, cracked corn, malted barley, and rye grain—and follow these steps:

  • Step 1: Sanitize all equipment, including your fermentation bucket and stirring spoon, using a food-grade sanitizer solution to prevent contamination.
  • Step 2: Heat 3 gallons of filtered water in a large stock pot to 145°F (63°C), then add 5 pounds of cracked corn, 2 pounds of malted barley, and 1 pound of rye grain. Stir thoroughly to combine.
  • Step 3: Maintain the temperature for 90 minutes to allow enzymes to convert starches into fermentable sugars, creating a rich, sweet base that enhances the final moonshine’s smooth profile.
  • Step 4: Cool the mixture rapidly to below 70°F (21°C) using an ice bath or chiller, then transfer it to a sanitized fermentation bucket. Cover and store in a cool, dark place for up to 24 hours.

Fermenting in Advance

Fermentation is a critical stage where yeast transforms sugars into alcohol, and doing this ahead can save time before distillation. We advise fermenting your mash 7–10 days in advance, but monitor it closely to avoid off-flavors.

Here’s how to proceed safely:

  • Step 1: Once your mash base is ready, pitch the distiller’s yeast (1 packet for a 5-gallon batch) and add yeast nutrient if needed for robust fermentation.
  • Step 2: Seal the bucket with an airlock and stopper, then place it in a stable environment at 68–72°F (20–22°C) for 5–7 days. Track the specific gravity daily using a hydrometer to ensure it drops from an initial reading of 1.050–1.070 to below 1.000, indicating completion.
  • Step 3: After fermentation, strain the liquid through a fine mesh to remove solids, then store the wash in a sanitized container in the refrigerator for up to 3 days. This chilling step preserves the fresh, fruity notes while halting yeast activity.

Storage and Safety Tips

Storing make-ahead components requires attention to detail to uphold quality and prevent risks. Use the following table to compare storage options based on what you’re preparing:

Component Recommended Storage Method Duration Key Considerations
Mash Base Airtight container in fridge Up to 24 hours Keep below 40°F (4°C) to avoid bacterial growth.
Fermented Wash Sealed, sanitized jug in fridge Up to 3 days Monitor for signs of spoilage, like off odors.
Distilled Moonshine Glass bottles in a cool, dark place Up to 6 months Age with oak chips for enhanced flavor, ensuring it’s proofed to 80–100.

Always prioritize sanitation and taste tests before proceeding—our goal is to deliver a confident, high-quality result every time. By planning ahead, we make your moonshine-making experience efficient and enjoyable.

Conclusion

We’ve guided you through crafting a 5 Gallon Moonshine Mash Recipe that’s safe and rewarding. By blending tradition with modern techniques, you’ll create spirits that bring people together.

Remember, quality ingredients and careful steps ensure the best results every time. We’re excited for you to enjoy your homemade moonshine responsibly—it’s a timeless craft we’re proud to share.

Frequently Asked Questions

What is moonshine and its history?

Moonshine is a homemade distilled spirit with roots in American ingenuity and rebellion, often made during prohibition to evade taxes. It’s a symbol of self-reliance, evolving from early settlers’ practices to modern home brewing.

What ingredients are needed for a 5-gallon moonshine mash?

You’ll need filtered water, cracked corn, malted barley, rye grain, distiller’s yeast, optional white sugar, and yeast nutrient. Use fresh ingredients to ensure proper fermentation and flavor—quantities are specified for a 5-gallon batch to promote quality and avoid contaminants.

What equipment is essential for making moonshine?

Key items include a fermentation bucket, airlock and stopper, hydrometer, thermometer, large stock pot, stirring spoon, strainer, and sanitizer solution. Choose food-grade equipment to prevent contamination and select based on batch size for safe, efficient brewing.

How do I prepare the moonshine mash?

Start by heating filtered water, adding grains like cracked corn, malted barley, and rye, then stir and cool the mixture. Sanitize all equipment first and maintain proper temperatures to ensure successful fermentation and flavor development.

What is the fermentation process for moonshine mash?

Fermentation involves pitching yeast into the cooled mash, where it converts sugars to alcohol over 7-10 days. Monitor with a hydrometer to track specific gravity, keep temperatures ideal, and ensure a sanitary environment for a smooth, flavorful result.

How do I distill moonshine safely?

Set up your still, heat the fermented mash, and collect the distillate, separating it into heads, hearts, and tails for best flavor. Always prioritize safety by using proper equipment, monitoring temperatures, and discarding unsafe portions before aging.

Can I make moonshine ahead of time?

Yes, prepare the mash base up to 24 hours in advance and ferment 7-10 days ahead. Cool and store the mash properly in sanitized containers, then distill when ready to streamline the process while maintaining quality and safety.